Cannabidioli (CBD) isomeerumine psühhoaktiivseteks kannabinoididideks

[MuricanSpirit]

Nii et ma segasin nüüd 20g toidusoodat (ma panin niikuinii enne ära, nii et miks mitte jätkata). Segasin seda umbes 1h segamispulgaga. Etanooli ei olnud piisavalt, et eralduda, seega lisasin (enne segamist) 40ml etanooli.

Eemaldasin pealmise kihi süstlaga - naljakas, see oli lõpuks 50ml, nii et umbes 13ml on ikka veel sooda - ja viskasin selle keedukannu (madalaim kuumutuskoht 56°).

Suitsetan seda paska varsti. Lõhnab ikka veel, aga palju paremini kui varem.

 

[mycelium]

Just so you know, after the reaction, it is distilled again or maybe twice, in order to clean it up and remove reaction byproducts

 

[WillD]

Tavaliselt sobib puhas CBD-pulber isomeriseerimiseks, ma ei tea, kui puhtaks protsess läheb õliga

 

[mycelium]

I think anyone who is making it for sales should use isolate, and DISTILL END PRODUCT AT LEAST ONE TIME

 

[PossumKid]

Kas te saate küsida, mis puhtusastmega on tegemist?
Tavaliselt, kui see on isolaat, peaks see olema hea, kuid asjaolu, et seal on kirjas ka "laia spektriga", ajab mind veidi segadusse.

 

[mycelium]

Broad spectrum means all cannabinoids, not isolated like CBD isolate

 

[Kvadprime]

I love vape with TGK ... I think I can do:

1. Start reaction in ethanol with acetic acid for 12-24h.
2. After - we evaporate all the ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?

 

[WillD]

You do not have to evaporate it. You can dilute with water and separate the oil if you use ethanol.

 

[Kvadprime]

Ok! I try to do it, thx!!

But 5g cbd in my town i cant get with good price for first try

I try with 1g cbd in 10ml ethanol with ~1ml AcOH

Thx!!!!!!!

 

[WillD]

The reaction time can be a little longer than we wrote before. You need to examine to choose the best time if you do not have the opportunity to make an analyst.

 

[Rafa]

what substitutes can i use for Et2O?

 

[WillD]

We need more details to a specific task.

 

[Rabidreject]

Yeah, I’m probably going to end up just running it a few diff ways, I said HCl purely because I have some lol
I saw someone synthesise some p-tsa the other day and it was far less violent than I’d expected so I’ll probably whip some of that up and also give the citric acid method a go also.

 

[Rabidreject]

In terms of vacuum distilling out the product for purification, I assume I’ll be able to vacuum distil to separate the d9 and d8 right? If I use a collumn?

 

[mycelium]

@Rabidreject No sir, they come out at same temp.
It's damn near impossible, even with chromatography and lots of solvent, and this is from the professionals over at future