Cannabidioli (CBD) isomeerumine psühhoaktiivseteks kannabinoididideks

[kitboy]

Ma keetsin CBD-d ja lisasin kogemata segule NAoh, ma arvan, et isomeerumine peatus. Tekkis 2 kihti, kas keegi oskab öelda, mis tekkis? Kas see on hea viis THC ekstrakti ekstraheerimiseks?

Kasutan metanooli ja HCL-i

 

[G.Patton]

Tere, millises etapis olete lisanud NaOH-i?

Vastuse võib anda HPLC-analüüs.

 

[kitboy]

Pärast 2 tundi kestnud isomeerumist tekkis õli, kuid sellel on ebameeldiv lõhn ja ma ei tea, kuidas seda puhastada.

 

[kitboy]

Naohi lisamisel eraldusid kaks faasi ja ma arvan, et reaktsioon peatus. Ma proovisin seda mitmel viisil pesta, kuid ma ei saa sellest halvast lõhnast lahti.

 

[cvvvxa]

alused teisendavad cbd(thc ei muutu) mõneks kinooni derivaadiks. ma usun, et selle eraldamiseks thc-st saab kasutada erinevaid lahusteid, kuid ma ei mäleta, millises kirjanduses seda ka kirjeldati, kuna see on roheline(eeldan), ka mõned taimsed impuriidid võivad oksüdeeruda.

 

[kitboy]

Kumb on parem äädikhape või soolhape? Mul on jäänud õli, millel on vastik lõhn, mida ma teen selle puhastamiseks või puhta cbd loas metanoolist ekstraheerimiseks

 

[cvvvxa]

toatemperatuuri tolueeni ja p-tolueen-sulfoonhapet saab kasutada peaaegu puhta delta 9 ja teiste lahustite kuumusega tulemuseks delta 8

 

[cvvvxa]

tolueeni võib olla raske eemaldada, kuid, 44h(48h annab veidi rohkem konversiooni, kuid umbes 10% delta8) segatud 10% ptsa ja piisavalt tolueeni lahustamiseks, siis töötlemine

 

[kitboy]

Kui lisate NAOH-ga küllastunud vett, et happele vastu töötada, ei saa ma seda kõike kõrvaldada, ja kui ma lisan liiga palju vett, muutub ülemine faas mustaks. Kuidas ma saan ekstraheerimist teha? Kuidas ma kõrvaldan happe lõhna? Proovisin puhastada destilleeritud veega, kuid see ei toiminud.

Ma vajan abi selles küsimuses palun

Millise PH väärtusega peaksin ma THC jätma? Kas ma võin THC puhastamiseks kasutada butaani või tolueeni?

 

[WillD]

Meetodid, milles kasutatakse katalüütilisi koguseid happed, on ennast paremini kehtestanud kui selles teemas. PTSA 10% mol DCMis (delta-8) või HCl 0,05% etanoolis (delta-9) abil.

 

[Dr. MMX]

võib kasutada teistsugust alkoholi kui etüülaklooli? võib-olla hoopis ipa?
kas võib kasutada hcl?

 

[Irving Langmuir]

Ma arvan, et nii kaua, kuni teie reaktiivid on lahustuvad. HCl võib kasutada happekatalüsaatorina.

 

[WillD]

The change of solvent and the amount of acid greatly changes the composition of the result

 

[kitboy]

I think it is better to use methanol

 

[Kvadprime]

I love vape with TGK ... I think I can do:

1. We carry out isomerization in ethanol with acetic acid for 12-24h.
2. After - we evolve all ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?

 

[Kvadprime]

I love vape with TGK ... I think I can do:

1. Start reaction in ethanol with acetic acid for 12-24h.
2. After - we evaporate all the ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?

 

[WillD]

You do not have to evaporate it. You can dilute with water and separate the oil if you use ethanol.

 

[Kvadprime]

Hmmm... Of course!
And question

If I use AcOH in concentration about of 70-80%, It get to start isomerisation?

Now.... I can't get or make 100% acetic acid((

 

[WillD]

Then you need 7.5 (70%) - 6.5 (80%) mL of acetic acid soln. per ~100mL of ethanol (approximately).
Excess ethanol is necessary for the reaction to go well.
The resulting solution will take 5-10 g of cbd powder, nothing more.
Heat up to 70*C and boil at least 2 hours.
Dilute with water and collect the resulting oil.
You can write us about your results after.

 

[Kvadprime]

Ok! I try to do it, thx!!

But 5g cbd in my town i cant get with good price for first try

I try with 1g cbd in 10ml ethanol with ~1ml AcOH

Thx!!!!!!!

 

[WillD]

The reaction time can be a little longer than we wrote before. You need to examine to choose the best time if you do not have the opportunity to make an analyst.

 

[Rabidreject]

I have wanted to do this for ages but have been holding off as I don’t have p-tsa, however, if d9 is generally done with a catalytic amount of HCl, that would be MUCH easier.
Is it literally a case of chucking it all in, letting it react for ages at RT (12-24h I think I heard), quenching, extracting?

Seeing as THC is by far the drug I use the most, it would make sense for edibles or whatever. Doubt I would want to vape it though. Never was a huge fan of vaping distillate as it just screws my tolerance.

It looks pretty easy though

 

[Kvadprime]

Yes, it looks simple. That's why I want to try it!.. I'll write when I do it, there will be another report

 

[WillD]

If you use HCl for conversion, then heating is required.