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using 85% phosphoric acid instead of H20 in a 1:1 ratio to ephedrine creates a more effective reaction, mix ephedrine with phosphorus and then dissolve it in heated phosphoric acid, temperature approx. 100 °C and add iodine in increments so that the last iodine is added around 130 °C and the reaction ends at 140-150 °C. open the condenser flask and blow off the remaining iodine. iodine in a 1:1 ratio to ephedrine. 45-60 minutes and it is ready for extraction
 
with hydroiodic and red phosphorus i was able to extract in just 2 hours and it raises as fuck it's just something else and wizzy i don't know how to explain it
 
using 85% phosphoric acid instead of H20 in a 1:1 ratio to ephedrine creates a more effective reaction, mix ephedrine with phosphorus and then dissolve it in heated phosphoric acid, temperature approx. 100 °C and add iodine in increments so that the last iodine is added around 130 °C and the reaction ends at 140-150 °C. open the condenser flask and blow off the remaining iodine. iodine in a 1:1 ratio to ephedrine. 45-60 minutes and it is ready for extraction
This method carry great risk of explosion, once when i was young i tried to hydroiodic acid by mixing iodine and phosphoric acid (85%) and heating it and it exploded, so reaction is way safer with water, phosphorus acid is by product in the reaction and contribute nothik, by the way its intresting how they prepared phosphrous triiodide in situ to halogenate the OH group and reaction time decresed a lot, back in the days i was using 72h LWR to get the same output, Good video
 
How can I download it faster so I can watch it without lags. Or at least download it without it stopping automatic
 
with hydroiodic and red phosphorus i was able to extract in just 2 hours and it raises as fuck it's just something else and wizzy i don't know how to explain it
mate why use phosphorus if u use HI directly the poor phosphorus its precius care for the phosphorus like its ur kid or left nut :D
 
This method carry great risk of explosion, once when i was young i tried to hydroiodic acid by mixing iodine and phosphoric acid (85%) and heating it and it exploded, so reaction is way safer with water, phosphorus acid is by product in the reaction and contribute nothik, by the way its intresting how they prepared phosphrous triiodide in situ to halogenate the OH group and reaction time decresed a lot, back in the days i was using 72h LWR to get the same output, Good video
I have done this reaction 1000 times, while observing the proportions and reaction conditions, including the procedure of adding reagents and iodine in parts, nothing has ever happened to me
 
using 85% phosphoric acid instead of H20 in a 1:1 ratio to ephedrine creates a more effective reaction, mix ephedrine with phosphorus and then dissolve it in heated phosphoric acid, temperature approx. 100 °C and add iodine in increments so that the last iodine is added around 130 °C and the reaction ends at 140-150 °C. open the condenser flask and blow off the remaining iodine. iodine in a 1:1 ratio to ephedrine. 45-60 minutes and it is ready for extraction
Isn't phosphine produced at around 130-140 degrees?
 
I have done this reaction 1000 times, while observing the proportions and reaction conditions, including the procedure of adding reagents and iodine in parts, nothing has ever happened to me
jak říkáš... naše česká cesta se úplně obejde bez posraný vody :D.. m
 
This remains my best method but I don't do all this process like reduction for 24hours and it's very safe no risk, my only problem is getting ephedrine Hcl,
 
Yeah, when they took our premade HI, and we figured out making it with the P Phed in the flask, it cut a long cook down to 24 hours. They say if flashed right, its done in 3 hours. I always ran it 24
This method carry great risk of explosion, once when i was young i tried to hydroiodic acid by mixing iodine and phosphoric acid (85%) and heating it and it exploded, so reaction is way safer with water, phosphorus acid is by product in the reaction and contribute nothik, by the way its intresting how they prepared phosphrous triiodide in situ to halogenate the OH group and reaction time decresed a lot, back in the days i was using 72h LWR to get the same output, Good vide
 
But jesusjames do u know much about synthesis ephedrine or have u tried extracting ephedrine from pills does it actually give sharp big crystals like ephedrine Hcl, please lets share ideas and knowledge a little and permit me to call u teacher I joined this business 3years ago
 
My knowledge is no good anymore. It was 25 years ago when ephedrine was easy to get. At one time, I was able to walk into Costco and load up a shopping cart full of pills that extracted easily. My teacher would order cases af them and send me in to pick them up. He had a business licence for health food or something. I don't know cutting edge current info. Methods evolve with current issues. I'm using bmk glycidate and pmk glycidate. But I have been retired for the last 15 years. 10 of that was in prison. This is ot a game. Be careful.
But jesusjames do u know much about synthesis ephedrine or have u tried extracting ephedrine from pills does it actually give sharp big crystals like ephedrine Hcl, please lets share ideas and knowledge a little and permit me to call u teacher I joined this business 3years ago
 
i have the iodine reagent grade and red phosphorous, i just cant get these pills clean enough for a reaction. can somebody help me i got the pills alcohol washed then water washed then froze the water then filtered that. it looks like nothing but. pinwheels on a mirror. do yall think its good enough to react yet? they're the red pills the 30mg.
 

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Synthesis of Amphetamines (Phenylethylamines)
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