Isomerizace kanabidiolu (CBD) na psychoaktivní kanabinoidy

[MuricanSpirit]

Takže jsem teď smíchal 20 g potravinářské sody (stejně jsem to předtím posral, tak proč nepokračovat). Míchal jsem to míchadlem asi 1h. Ethanolu nebylo tolik, aby se oddělil, tak jsem přidal (před mícháním) 40ml Ethanolu.

Stříkačkou jsem odstranil vrchní vrstvu - vtipné, nakonec to bylo 50ml, takže asi 13ml je stále uvízlých v sodě - a hodil jsem to do hrnce na vaření (nejnižší bod ohřevu 56°).

Brzy to vykouřím. Pořád to smrdí, ale mnohem líp než předtím.

 

[mycelium]

Just so you know, after the reaction, it is distilled again or maybe twice, in order to clean it up and remove reaction byproducts

 

[WillD]

Obvykle se čistý prášek CBD hodí k izomerizaci, nevím, jak čistý proces probíhá u oleje.

 

[mycelium]

I think anyone who is making it for sales should use isolate, and DISTILL END PRODUCT AT LEAST ONE TIME

 

[PossumKid]

Můžete se jich zeptat, o jakou čistotu se jedná?
Obvykle, pokud je to izolát, by to mělo být dobré, ale to, že je tam také napsáno "široké spektrum", mě trochu mate.

 

[mycelium]

Broad spectrum means all cannabinoids, not isolated like CBD isolate

 

[Kvadprime]

I love vape with TGK ... I think I can do:

1. Start reaction in ethanol with acetic acid for 12-24h.
2. After - we evaporate all the ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?

 

[WillD]

You do not have to evaporate it. You can dilute with water and separate the oil if you use ethanol.

 

[Kvadprime]

Ok! I try to do it, thx!!

But 5g cbd in my town i cant get with good price for first try

I try with 1g cbd in 10ml ethanol with ~1ml AcOH

Thx!!!!!!!

 

[WillD]

The reaction time can be a little longer than we wrote before. You need to examine to choose the best time if you do not have the opportunity to make an analyst.

 

[Rafa]

what substitutes can i use for Et2O?

 

[WillD]

We need more details to a specific task.

 

[Rabidreject]

Yeah, I’m probably going to end up just running it a few diff ways, I said HCl purely because I have some lol
I saw someone synthesise some p-tsa the other day and it was far less violent than I’d expected so I’ll probably whip some of that up and also give the citric acid method a go also.

 

[Rabidreject]

In terms of vacuum distilling out the product for purification, I assume I’ll be able to vacuum distil to separate the d9 and d8 right? If I use a collumn?

 

[mycelium]

@Rabidreject No sir, they come out at same temp.
It's damn near impossible, even with chromatography and lots of solvent, and this is from the professionals over at future