PMK Oil Synthesys From PMK (CAS 28578-16-7 Wax Form) Large Scale

[btcboss2022]

Both have the same behaviour but powder is more clean or pure if you prefer ;-)

 

[Selassi]

I also hear the yellow waxy one has less yield, but we will see after test

 

[Bennyboy88]

The powder u had was white or yellowish in color I notice the separation of the oil is flowing on top. Is that because u used phos acid???.

 

[btcboss2022]

Hello,

Ratio, temperature and timing of NaHCO3 route please?
Thanks.

 

[G.Patton]

These are already written in your post, I just added scheme in order to improve and clarify information.

 

[Bennyboy88]

If phos acid will works. Woukd citrus acid can work too. Any comments anyone.

 

[G.Patton]

Citric acid is weak, I'm not sure that it will work

 

[btcboss2022]

Hello,

Here is my last achievement make it to crystallize naturally in the molecular form of the crystal itself. More pure impossible!! ;-)
Seems handmade but trust me are naturally formed!

 

[Tweaker]

Very nice work. What process do you use to remove the black tar like impurity? Even on snow white crystals it appears on subsequent recrystalizations and the end product becomes quite dark.

 

[btcboss2022]

Yes exactly the same.

 

[Paranoia]

Coming next in a few weeks @btcboss2022 ice sample lab test https://analisis2.energycontrol.org/ for meth purity and eniantometer R.S

 

[Bartholomeus]

What is this? Mdma Hcl ?

 

[btcboss2022]

Of course

 

[Bartholomeus]

Never seen such pure mdma thats why i ask, nice

 

[btcboss2022]

Me either until now ;-)

 

[Gale]

One of my very early synths, back when it only made sense to make product of this purity, but not very many people appreciate it for what it is..sadly.

This was back before when I did synths for a passion, being locked in labs told to make purple shit was whack.

 

[Mr Good Cat]

Most beautiful MDMA I've ever seen. Is it MDMA HCL? How you make it so transparent bro? I can make MDMA HCL pure white, not difficult. But still can achieve high transparency.

 

[Bennyboy88]

Well done btcboss2022. Nicest crystal I seen.

 

[Gale]

MDMA HCl -monohydrate
I moved towards making the anhydrous form, not as pretty but still similar looks

 

[Bennyboy88]

What method of crystallization you use to achieve these beauty. Do you mind sharing your method. Thx

 

[Gale]

I call these healing stones, for anyone wondering I used Dh20 and a gravity separation method I learned a while back inspired by JOR.

MDMA from 28578 yields a more dark brown or light yellow crystals via al/hg gassed

 

[btcboss2022]

Temp+Freeze Acetone+72hours freezer/Filter+water+temp+48 hours RT

 

[Bennyboy88]

What is the ratio of freebase:acetone. Your filtered starting powder have to be very clean in order to get clear crystal like at the end correct. Thx

 

[btcboss2022]

Hello freebase:acetone ratio is 1:10, I dont filtered the starting powder what you mean exactly?
Thanks.