1-Phenyl-2-nitropropene (P2NP) Video Synthesis From Benzaldehyde and Nitroethane. Henry Reaction.

HIGGS BOSSON

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Problems with nitroethane in Europe began back in 2007, then gradually all countries put restrictions on this valuable reagent. And now there are two ways: to look for suppliers in countries where there is weak legislation with a developed chemical industry, for example, Bangladesh, or to synthesize independently, the methodology for this we have proposed.
 

Alojz

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Wodurch kann man Nitroethan ersetzen oder selbst synthetisieren?
 

Kvadprime

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You can find methods of syntes nitroethane in another thread
 

Kvadprime

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I have aniline as a base - what yeilds can it give?
 

G.Patton

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Try and figure out. Share us your research data. In theory, it's quite weak base and it would be not enough to eliminate -OH group.
 

Kvadprime

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ok, I'll definitely write how everything went... I'm still waiting for my new labware to arrive

Thx
 

rampage

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has anyone done the microwave version of this synthesis, curious as to the outcome?
 
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