Isomerização do canabidiol (CBD) em canabinóides psicoativos

[MuricanSpirit]

Então, misturei agora 20 g de soda de grau alimentício (já tinha feito besteira antes, então por que não continuar). Misturei com uma barra de agitação por cerca de 1h. Não havia etanol suficiente para separar, então adicionei (antes de mexer) 40 ml de etanol.

Removi a camada superior com uma seringa - engraçado, acabou sendo 50 ml, então cerca de 13 ml ainda estão presos na soda - e joguei-a em uma panela (ponto de aquecimento mais baixo, 56°).

Vou fumar essa porcaria em breve. Ainda está cheirando mal, mas muito melhor do que antes.

 

[mycelium]

Just so you know, after the reaction, it is distilled again or maybe twice, in order to clean it up and remove reaction byproducts

 

[WillD]

Normalmente, o pó puro de CBD se presta à isomerização, mas não sei o grau de pureza do processo com o óleo

 

[mycelium]

I think anyone who is making it for sales should use isolate, and DISTILL END PRODUCT AT LEAST ONE TIME

 

[PossumKid]

Você pode perguntar a eles qual é a pureza do produto?
Normalmente, se for isolado, deve ser bom, mas o fato de também dizer "amplo espectro" me confunde um pouco.

 

[mycelium]

Broad spectrum means all cannabinoids, not isolated like CBD isolate

 

[Kvadprime]

I love vape with TGK ... I think I can do:

1. Start reaction in ethanol with acetic acid for 12-24h.
2. After - we evaporate all the ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?

 

[WillD]

You do not have to evaporate it. You can dilute with water and separate the oil if you use ethanol.

 

[Kvadprime]

Ok! I try to do it, thx!!

But 5g cbd in my town i cant get with good price for first try

I try with 1g cbd in 10ml ethanol with ~1ml AcOH

Thx!!!!!!!

 

[WillD]

The reaction time can be a little longer than we wrote before. You need to examine to choose the best time if you do not have the opportunity to make an analyst.

 

[Rafa]

what substitutes can i use for Et2O?

 

[WillD]

We need more details to a specific task.

 

[Rabidreject]

Yeah, I’m probably going to end up just running it a few diff ways, I said HCl purely because I have some lol
I saw someone synthesise some p-tsa the other day and it was far less violent than I’d expected so I’ll probably whip some of that up and also give the citric acid method a go also.

 

[Rabidreject]

In terms of vacuum distilling out the product for purification, I assume I’ll be able to vacuum distil to separate the d9 and d8 right? If I use a collumn?

 

[mycelium]

@Rabidreject No sir, they come out at same temp.
It's damn near impossible, even with chromatography and lots of solvent, and this is from the professionals over at future