Isomérisation du cannabidiol (CBD) en cannabinoïdes psychoactifs

[MuricanSpirit]

J'ai donc mélangé maintenant 20g de soude alimentaire (j'ai merdé de toute façon avant, alors pourquoi ne pas continuer). J'ai mélangé le tout avec une barre d'agitation pendant environ 1h. Il n'y avait pas assez d'éthanol pour le séparer, j'ai donc ajouté (avant de remuer) 40ml d'éthanol.

J'ai enlevé la couche supérieure à l'aide d'une seringue - c'est drôle, ça a fini par faire 50ml, donc environ 13ml sont encore coincés dans la soude - et je l'ai jeté dans une marmite (point de chauffe le plus bas 56°).

Je vais bientôt fumer cette merde. Ca sent toujours aussi bon mais c'est encore mieux qu'avant.

 

[mycelium]

Just so you know, after the reaction, it is distilled again or maybe twice, in order to clean it up and remove reaction byproducts

 

[WillD]

En général, la poudre pure de CBD se prête à l'isomérisation, mais je ne sais pas à quel point le processus est pur pour l'huile.

 

[mycelium]

I think anyone who is making it for sales should use isolate, and DISTILL END PRODUCT AT LEAST ONE TIME

 

[PossumKid]

Pouvez-vous leur demander de quelle pureté il s'agit ?
En général, s'il s'agit d'un isolat, cela devrait aller, mais le fait qu'il soit également indiqué "large spectre" me perturbe un peu.

 

[mycelium]

Broad spectrum means all cannabinoids, not isolated like CBD isolate

 

[Kvadprime]

I love vape with TGK ... I think I can do:

1. Start reaction in ethanol with acetic acid for 12-24h.
2. After - we evaporate all the ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?

 

[WillD]

You do not have to evaporate it. You can dilute with water and separate the oil if you use ethanol.

 

[Kvadprime]

Ok! I try to do it, thx!!

But 5g cbd in my town i cant get with good price for first try

I try with 1g cbd in 10ml ethanol with ~1ml AcOH

Thx!!!!!!!

 

[WillD]

The reaction time can be a little longer than we wrote before. You need to examine to choose the best time if you do not have the opportunity to make an analyst.

 

[Rafa]

what substitutes can i use for Et2O?

 

[WillD]

We need more details to a specific task.

 

[Rabidreject]

Yeah, I’m probably going to end up just running it a few diff ways, I said HCl purely because I have some lol
I saw someone synthesise some p-tsa the other day and it was far less violent than I’d expected so I’ll probably whip some of that up and also give the citric acid method a go also.

 

[Rabidreject]

In terms of vacuum distilling out the product for purification, I assume I’ll be able to vacuum distil to separate the d9 and d8 right? If I use a collumn?

 

[mycelium]

@Rabidreject No sir, they come out at same temp.
It's damn near impossible, even with chromatography and lots of solvent, and this is from the professionals over at future