Isomerización del cannabidiol (CBD) en cannabinoides psicoactivos

[MuricanSpirit]

Así que mezclé ahora 20g de sosa alimentaria (ya la había cagado antes, así que por qué no continuar). Lo mezclé con una barra agitadora durante aproximadamente 1h. No había suficiente etanol para separar así que añadí (antes de agitar) 40ml de etanol.

Quité la capa superior con una jeringuilla - curioso, al final fueron 50ml así que unos 13ml siguen pegados en la sosa - y lo eché en una olla (punto de calentamiento más bajo 56°).

Voy a fumar esa mierda muy pronto. Todavía huele, pero mucho mejor que antes.

 

[mycelium]

Just so you know, after the reaction, it is distilled again or maybe twice, in order to clean it up and remove reaction byproducts

 

[WillD]

Por lo general, el polvo puro de CBD se presta a la isomerización, no sé cómo de puro es el proceso con el aceite

 

[mycelium]

I think anyone who is making it for sales should use isolate, and DISTILL END PRODUCT AT LEAST ONE TIME

 

[PossumKid]

¿Puede preguntarles de qué pureza se trata?
Normalmente, si se trata de un aislado, debería estar bien, pero el hecho de que también diga "amplio espectro" me confunde un poco.

 

[mycelium]

Broad spectrum means all cannabinoids, not isolated like CBD isolate

 

[Kvadprime]

I love vape with TGK ... I think I can do:

1. Start reaction in ethanol with acetic acid for 12-24h.
2. After - we evaporate all the ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?

 

[WillD]

You do not have to evaporate it. You can dilute with water and separate the oil if you use ethanol.

 

[Kvadprime]

Ok! I try to do it, thx!!

But 5g cbd in my town i cant get with good price for first try

I try with 1g cbd in 10ml ethanol with ~1ml AcOH

Thx!!!!!!!

 

[WillD]

The reaction time can be a little longer than we wrote before. You need to examine to choose the best time if you do not have the opportunity to make an analyst.

 

[Rafa]

what substitutes can i use for Et2O?

 

[WillD]

We need more details to a specific task.

 

[Rabidreject]

Yeah, I’m probably going to end up just running it a few diff ways, I said HCl purely because I have some lol
I saw someone synthesise some p-tsa the other day and it was far less violent than I’d expected so I’ll probably whip some of that up and also give the citric acid method a go also.

 

[Rabidreject]

In terms of vacuum distilling out the product for purification, I assume I’ll be able to vacuum distil to separate the d9 and d8 right? If I use a collumn?

 

[mycelium]

@Rabidreject No sir, they come out at same temp.
It's damn near impossible, even with chromatography and lots of solvent, and this is from the professionals over at future