Изомеризация на канабидиола (CBD) до психоактивни канабиноиди

[MuricanSpirit]

И така, сега смесих 20 г сода за хранителни цели (така или иначе се прецаках преди, така че защо да не продължа). Разбърквах я с бъркалка в продължение на около 1 ч. Нямаше достатъчно етанол, за да се отдели, така че добавих (преди разбъркването) 40ml етанол.

Отстраних горния слой със спринцовка - смешно, в крайна сметка той беше 50ml, така че около 13ml все още са заседнали в содата - и го хвърлих в тенджера за готвене (най-ниска точка на нагряване 56°).

Съвсем скоро ще пуша тази гадост. Все още мирише, но много по-добре от преди.

 

[mycelium]

Just so you know, after the reaction, it is distilled again or maybe twice, in order to clean it up and remove reaction byproducts

 

[WillD]

Обикновено чистият CBD прах се поддава на изомеризация, не знам колко чист е процесът при маслото

 

[mycelium]

I think anyone who is making it for sales should use isolate, and DISTILL END PRODUCT AT LEAST ONE TIME

 

[PossumKid]

Можете ли да ги попитате каква е чистотата му?
Обикновено, ако е изолат, би трябвало да е добре, но фактът, че пише и "широк спектър", малко ме обърква.

 

[mycelium]

Broad spectrum means all cannabinoids, not isolated like CBD isolate

 

[Kvadprime]

I love vape with TGK ... I think I can do:

1. Start reaction in ethanol with acetic acid for 12-24h.
2. After - we evaporate all the ethanol and acetic acid
3. Pour the resin with a mixture of glycerol and propylene glycol, dissolving gravs completely
4. Pour into a comfortable jar and smoke

The issue of health safety - alcohol and acetic acid should clearly not be synthetic - only food (We make THC from the CBD using trembling and sugar, aahahhaha)

Experienced isomerization specialists - what do you think? Is it worth a try?

 

[WillD]

You do not have to evaporate it. You can dilute with water and separate the oil if you use ethanol.

 

[Kvadprime]

Ok! I try to do it, thx!!

But 5g cbd in my town i cant get with good price for first try

I try with 1g cbd in 10ml ethanol with ~1ml AcOH

Thx!!!!!!!

 

[WillD]

The reaction time can be a little longer than we wrote before. You need to examine to choose the best time if you do not have the opportunity to make an analyst.

 

[Rafa]

what substitutes can i use for Et2O?

 

[WillD]

We need more details to a specific task.

 

[Rabidreject]

Yeah, I’m probably going to end up just running it a few diff ways, I said HCl purely because I have some lol
I saw someone synthesise some p-tsa the other day and it was far less violent than I’d expected so I’ll probably whip some of that up and also give the citric acid method a go also.

 

[Rabidreject]

In terms of vacuum distilling out the product for purification, I assume I’ll be able to vacuum distil to separate the d9 and d8 right? If I use a collumn?

 

[mycelium]

@Rabidreject No sir, they come out at same temp.
It's damn near impossible, even with chromatography and lots of solvent, and this is from the professionals over at future