MDMA/ecstasy purification method

[K53SK53S]

Hello friends, thanks for the contribution, it works very well but I have a doubt, when crystallizing (crystals precipitate very very well) I do not get crystals like the typical ones of mdma, it is something more similar to snowflakes, to ice frost in a glass on a snowy day, it is glass but very fragile. Why can't I get strong glass? Thank you and greetings

 

[G.Patton]

Hi, you are welcome! Do you use a fridge for the crystallization procedure? The faster cooling down, the smaller crystals.

 

[K53SK53S]

Yes, of course, first I leave it out until it is at room temperature, then 15 or 20% has already crystallized, then I put it in the refrigerator for 2 hours and then in the freezer for 3 hours. Almost 100% of the washed product crystallizes, but the crystals are very fragile, when handled for packaging they turn into sand

 

[Mr Good Cat]

I did IPA a few times, and I guess this "sand" crystal style is a natural property of IPA crystallization. Try to recrystallize it in water to obtain big rock crystals.

 

[K53SK53S]

In water? How do you do it like that mate?

 

[Mr Good Cat]

http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/threads/my-mdma-freebase-crystallization.5069/

 

[Mr Good Cat]

What I noticed, IPA is good to remove sticky black compound, side product of synth.

 

[William D.]

Large crystals are obtained with the inclusion of a water molecule. Therefore, sometimes it is better to use aq. HCl acid or add water additionally. You must begin crystallization at room temperature so that the process does not begin quickly. If you show a photo of your crystals, maybe I will tell you that you can change for this and get it in a larger size.