Nitroetan Vir

[InLikeFlynn]

Pravzaprav sem našel stekleničko tega za svoj sintetizator P2NP. Zdaj potrebujem le še N-butilamin (s tem imam nekaj težav).

 

[FENTAMAS]

Uporabite lahko tudi druge amine, na primer izobutilamin, ki ga zlahka dobite z dekarboksilacijo a-aminokislin valina.

 

[Macondor]

Hvala, sprašujem, ker je to..
"Raztopite 140 g (1 mol) heksametilentetramina (urotropin, heksamin) in 157,5 g (1,05 mola) natrijevega jodida (ali 174 g (1,05 mola) kalijevega jodida) v 1000 ml vročega 95 % etilnega alkohola (190-odstotni žitni alkohol). Nato dodamo 243 g bromosafrola (1 mol) in raztopino pustimo stati, dokler ne pride do obarjanja. Nato v zmes spustimo tok plinastega HCl, kjer se oborina hidrolizira, raztopi in izloči amonijev klorid. Amonijev klorid filtriramo in alkohol iz filtrata odstranimo z destilacijo pod znižanim tlakom. Surovi amin, ki ostane, očistimo tako, da sprostimo prosto bazo z raztopino NaOH (45 g NaOH v 135 ml vode). Olje ekstrahiramo z etrom (ali toluenom, metilen kloridom itd.) in ga ponovno pretvorimo v HCl sol s tokom HCl plina. Kristale, ki nastanejo iz etra, filtrirajte."

 

[yuiopjkl]

Ta izdelek me je zanimal že prej, po raziskovanju pa sem prebral, da vsebuje 99 % nitroetana ( varnostni list ).
Vendar sem nekje na internetu prebral, da ga je nekdo preizkusil in dejal, da vsebuje le majhno količino nitroetana (mislim, da 10 %).

 

[InLikeFlynn]

Zanima me, ali so uporabili "korak 6" in ne drugega koraka v tej družini izdelkov. AFAIK je korak 6 edini, ki je v prvi vrsti nitroetan. Korak 8 vsebuje aceton in nitroetan.


"Cuccio Pro Powder Polish Dip System Step 8 Dipping Powder Remover"
Kemijsko ime masni % CAS št.
ACETON 60-75 % 67-64-1
NITROETAN 25-40 % 79-24-3

 

[BalkanBoys]

go to universalcompanies dot come site there is the exact product and it says 99% nitroethane in the official technical sheet. I'm ordering, let's see.

 

[SoldadoDeDrogas]

I was looking into a product for my own usage. I came across one on ebay called Mia Secret Brush Conditioner, they were 30ml bottles with nitroethane as the main ingredient. Turns out this was the old formula. The ingredient substituted now is 1-nitropropene, so I believe I hit a dead end here.

Anybody have any suggestions? I've been trying to get to p2np for over a year now, but I haven't had any luck coming up with the propene.

 

[mycelium]

From diethylamine sulfate and sodium nitrite, both available online

 

[mycelium]

 

[mycelium]

Diethyl sulfate, I can't believe autocorrect put in diethylamine...

 

[SoldadoDeDrogas]

Phone has ergot on it's agenda ;]

 

[SoldadoDeDrogas]

Phone has ergot on it's agenda ;]