Unele săruri de amfetamină

rampage

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i did a p2np al/hg amination to amphetamine, but when i finished i ended up with an oil, i did not gas it with hcl i just added hydrochloric acid with acetone and dripped it into rm until i reached a ph of 6, ive tried evaporating it and just end up with an oil, and i want to get amph hcl. any suggestions on what to do would be appreciated?
 

GhostChemist

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Precipitation of an amphetamine with H2SO4 or H3PO4 give a powders.
But amphetamine with HCl solution with acidic pH (better 3-4) should be evaporated to precipitate and dried in desiccator contains NaOH
 
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rampage

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thanks for your advice mate
 
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