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JWH-018 synthesis. Small scale.

Bigwest

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I have all the ingredients, i am trying to Split the 8 & 4 minutes of irradiation on 2 by 2 minutes and let thé product cooled between them but its not working. Could somone help with that pls.
 

G.Patton

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You can try to split it to 10-25 sec. Don't cool them too much.
 
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Bigwest

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Hi
I did check all the melting points of my raw material. Evry thing its OK. Have you try this synthesis by à household microwave ?

I think its not gonna working. it Just can be done by a mw reactor only
 

G.Patton

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Hi, I didn't. I asked about this synthesis for you from William. Ty for your feedback.
 

Bigwest

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I write to william in pm. I hope hé gonna reply. But i am sûre that Theres somthing wrong.
 

Nicky

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Hello.. Just a little explication pleas.
How long should we irradiate the product when using a home microwave---8--4 minutes or 10---25-- seconds? And does the cup have to be closed?
 

Nicky

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Do we use 400w also in household microwave ?
 

41Dxflatline

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If microwaves work then so should ultrasound
 

Alex7920

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What type of microwave is good for this reaction? Can this reaction be done with a home microwave?
 

joejoe354354

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Hello,I would like to ask if this method is nof suitable for mass production?
 

HerrHaber

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This may only be possible with the aid of a flow type MW reactor that can be conceived as improvisable from a household device but needs someone with quite some experience and balls.
 

pakanahesa

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Hello bro, Greetings to you master. Its small scale for light dose or strong dose? Thx. Coz i try it 1st its not effect at all
 

WillD

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2-3mg per one hit. u can make a reaction in stages that check each stage for success.
 

robloxgelap

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all the ingredients are easily available, but making it looks difficult. is there anyone who can help me? especially for steps 6, 7, and 8 how to filter aluminum oxide, what is the temperature for reflux, and what is the aluminum oxide filtered and then washed for? because in the next step aluminum oxide is not mentioned that it will be used again.
 

soebunies

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@robloxgelap aluminium oksida ga larut dalam etanol, suhu reflux adalah suhu titik didih pelarut, tujuan pencucian aluminium oksida agar bisa digunakan kembali di reaksi berikutnya
 
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robloxgelap

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berarti untuk membuat kembali jwh, ga perlu beli alumunium oksida lagi? dan bisa pake alumunium oksida yang sebelumnya udah pernah dipakai dan sudah di cuci?
 

soebunies

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benar, hati hati sama asep kuning yang keluar, harus selalu dipantau ya👍
 

mycelium

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I don't understand people not being able to hear EtOH in the microwave
Or maybe around here everyone has cannabis oil and makes candy and shit.
Microwaves have lights inside.
With 50ml ethanol, I hear it for 15 seconds which is normally enough to make it real warm.
Then short bursts, and looking at the beaker in the microwave.
The slightest bubbles and you stop , because it goes from a couple bubbles to over boiling almost instant.
 
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