Nitroethane Source

[InLikeFlynn]

I actually found a bottle of this for my P2NP synth. All I need is N-butylamine now (having some trouble on that front)

 

[FENTAMAS]

You can use other amines too, for example Isobutylamine, that is easy obtainable via Valine a-amino acid decarboxylation.

 

[Macondor]

thanks, i ask because this..
"Dissolve 140g (1 mole) of hexamethylenetetramine (urotropine, hexamine) and 157.5g (1.05 moles) sodium iodide (or 174g (1.05 moles) potassium iodide) in 1000ml of hot 95% ethyl alcohol (190 proof grain alcohol). 243g of bromosafrole (1 mole) is then added and the solution is allowed to stand until no precipitation occurs. A stream of HCl gas is then run into the mixture where the precipitate is hydrolyzed, dissolves and ammonium chloride precipitates. The ammonium chloride is filtered off and the alcohol of the filtrate is removed through distillation under reduced pressure. Purify the crude amine left by releasing the free base with NaOH solution (45g NaOH in 135 ml water). Extract the oil with ether (or toluene, methylene chloride etc.) and reconvert to the HCl salt with a stream of HCl gas. Filter the crystals formed from the ether."

 

[yuiopjkl]

I was interested in this product before and after researching I read that it contains 99% nitroethane ( Material safety data sheet )
But I read somewhere on the internet that someone had tried it and said it only contained a small amount of nitroethane (I think 10%).

 

[InLikeFlynn]

I'm curious if they used "Step 6" and not another step in this family of products. AFAIK Step 6 is the only one that is primarily nitroethane. Step 8 has Acetone and Nitroethane.


"Cuccio Pro Powder Polish Dip System Step 8 Dipping Powder Remover"
Chemical Name % by Weight CAS #.
ACETONE 60-75% 67-64-1
NITROETHANE 25-40% 79-24-3

 

[BalkanBoys]

go to universalcompanies dot come site there is the exact product and it says 99% nitroethane in the official technical sheet. I'm ordering, let's see.

 

[SoldadoDeDrogas]

I was looking into a product for my own usage. I came across one on ebay called Mia Secret Brush Conditioner, they were 30ml bottles with nitroethane as the main ingredient. Turns out this was the old formula. The ingredient substituted now is 1-nitropropene, so I believe I hit a dead end here.

Anybody have any suggestions? I've been trying to get to p2np for over a year now, but I haven't had any luck coming up with the propene.

 

[mycelium]

From diethylamine sulfate and sodium nitrite, both available online

 

[mycelium]

 

[mycelium]

Diethyl sulfate, I can't believe autocorrect put in diethylamine...

 

[SoldadoDeDrogas]

Phone has ergot on it's agenda ;]

 

[SoldadoDeDrogas]

Phone has ergot on it's agenda ;]