MDP2NP Full Synthesis From Natural Piperine

[ukises]

I got piperonal obtained Via ozonolysis,How can I purify it? Thanks

 

[mycelium]

Hey, @ukises what ozone machine did you use? I read about this reaction last week

 

[ukises]

This one

 

[ukises]

This one Ozone 2000/ hour

 

[mycelium]

Thank you

 

[ukises]

Why the your piperonal still in liquid, and not crystals form?

 

[GhostChemist]

Because the obtained piperonal has such physical and chemical properties and environmental conditions

 

[ukises]

Hello Master I got all.the reagents and materials , maybe you can tellme the necesary quantity for make 100 grams, thanks

 

[G.Patton]

Hello, you can calculate them proportionately in accordance with this method.

 

[ukises]

You mean for 100 grs piperine 2 liters thf, 4 liters solution potassium permanganate

 

[ukises]

Nice job, thanks , i got 5 kgs piperine i want piperonal,but this way is for small scale