Synthesis of 5cl-adbb

[Voldermort101]

Hi I am currently trying to synthesis 5cl-adbb. I was given the instructions below. However I seem to be having issues. When I filter the liquid , nothing is being filtered via the filter paper. The Pottasium Carbonate does dissolve with the addition of cold water. However extraction of final product is impossible as the golden brown liquid just passes through the filter without leaving any final product. Any help would be appreciated.

1) ADBB precursor (main material)
2) Three auxiliary material:
DMF ( Cas: 68-12-2 )
Anhydrous Pottasium Carbonate ( Cas: 584-08-7)
Bromobutane ( Cas: 109-65-9 )

3) Tools:
Stainless Steel or Glass Reaction Bottle with stirring and heating function
PH Detector and disposable filter paper
Buchner Funnel;vaccum filtration kit;vacuum pump

 

[Ecko6ap]

bro, tell me where you bought the precursor?

 

[sirmtr]

You have adbb recipe to make
Bromobutane you will make for sure adbb

 

[Voldermort101]

I'm getting an oily substance as final product. How do I get it to crystallize? Thanks

 

[Ecko6ap]

it is working?

 

[tucoXxX]

when you turn off the magnetic stirrer after 4 hours, prepare ice water (in a plastic bowl). I pour the reaction mixture into it slowly while stirring. Stirring for 5 minutes will be fine. I let it rest for 4 hours. I received a completely muddy product. I didn't have any filter paper. I bought oil filter paper €1 10 from a car store I filtered it twice. I waited 2 hours, I saw mud at the bottom of the glass flask and it didn't want to be a stone. I poured excess water. a bowl of mud remained. 10 hours passed and there was a big stone in the bowl. I once made 100g 5cladba precursor plus the reduced 3 ingredients (2 powder, 2 liquid). you have better equipment, I think you will succeed.....

 

[tucoXxX]

I simply poured off the excess water. I started with 100g 5c for the first time. I corrected my writing because my English is bad

 

[impressive-match-292]

Im in need of help with the finishing process of my raw material?

 

[Lipopoyy]

I can sent you complete tutorials on that
not free please

 

[PharmaTech4510]

Try This

 

[impressive-match-292]

Hi friend I'm having the same issue that you are having did you figure it out?