Today I will be updating my old rushed synthesis of the shake and bake. This will include proper glassware, equipment, washing of impurities, and recrystallization with additional purifications like cold anhydrous acetone washings!
Precursors needed with measurements:
10 grams of ephedrine or...
Introduction
I represent to BB audience Methamphetamine synthesis method of 1-phenyl-2-propanon (P2P) reductive amination by NaBH4. Following method allows obtaining and large batches of product. The hardest problem of this method is the heat generating during exothermic reaction of imine...
Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets.
Pseudoephedrine was extracted from Sudafed tablets using ethanol, ethanol/methanol (90:10% vol/vol) and methylated spirits. The solvents were chosen with reference to the relevant clandestine literature. For each extraction...