Hey there, this is Eumer. It's my first post on the forum so I apologize in advance if I'm missing out the rules or anything else.
I can buy camphor oil from my local stores which I heard that it contains safrole and camphor for sure. I need to seperate safrole from this oil but I don't know...
link to original synth here!! ^_^
4-allyl catechol really only serves one purpose - as an intermediate to synthetic safrole. It is a white to tan powder with a characteristic smell of diesel/smoke. Quick or easy are two words that should never describe the synthesis of 4-allyl catechol. While...
honestly i'm not exactly sure how this chemical is used in a safrole synth but a link containing a diiodomethane synth was found in a safrole synthesizing thread on the vespiary, so here u guys go ^^; hope someone can find use for this
Methylene chloride (30 grams) is mixed with sodium iodide...
synthesis by raffike from the vespiary :3
pls note that Fe(CO)5 is super toxic and "it's recommended to do the reaction under a fume hood or with good ventilation"
Reagents:
ᗢ 500 grams of safrole distilled from Ocotea Cymbarum
ᗢ 3 grams of technical +98,5%NaOH
ᗢ 3 grams of lab grade Fe(CO)5...
hey :3 i would copy-paste this like i usually do with vespiary stuff but theres a lot of info so i decided 2 leave it in link form. there are many syntheses and theyre easy 2 read and perfect for beginners. enjoy!
http://www.thevespiary.org/rhodium/Rhodium/hive/hiveboard/methods/000023325.html
here are 3 methods for the isolation of safrole i grabbed from here ^_^ check the link for references
Here are the first three references from TSII that deal with the purification of safrole from essential oils using another mercury salt, mercuric acetate [Mg(AcO)2]. Note than in TSII, Strike...
Where I live there is no source to get safrole other than piper auritum, with the advantage that this is a plague and it is everywhere, what you guys think about the synthesis of mdma from piper auritum oil, I am purifying the oil as shown in strike Total Synthesis, purification with 28% glacial...
Introduction
These precursors, are controlled or regulated substances in many jurisdictions. The use of uncontrolled precursors therefore offers clandestine laboratory operators a strategy to reduce the risk associated with detection. Catechol (1) is a common chemical reagent that is synthesized...