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pybop

  1. William D.

    LSD synthesis from lysergic acid via PyBOP

    Reagents: Lysergic acid (cas 82-58-6)2.80 g; Methylene chloride (DCM; CH2Cl2) 190 ml; N,N-Diethylmethylamine (cas cas 616-39-7) 1.81 g; PyBOP (cas 128625-52-5) 5.70 g; Diethylamine (cas 109-89-7) 0.84 g; Ammonium hydroxide (NH4OH) 100 ml 7.5 M; Sodium bicarbonate (cold saturated aq solution)...
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