p2p synthesis

I tried synthesizing P2P from P2NP using tin chloride dihydrate. Got organish yellow oil after quenching with water. When dcm was added it formed a turbid pale yellow mixture of dcm and p2p. I added methylamine to the mixture and then added aluminum and hcl to reduce it to methamphetamine free...

Acetophenone makes 1-phenyl-2-propanone (P2P) Material: Acetophenone (C6H5COCH3): 50 mL Methyl iodide (CH3I): 30 mL Potassium hydroxide (KOH): 10 g Ethanol or dimethyl sulfoxide (DMSO): 100 mL Steps and possible situations: Alkaline treatment: Operation: Dissolve 50 mL acetophenone in 100 mL...

seeking help

Chapter 1 Benzene Reagents 100 g Sodium Benzoate 0,877 mol (C7H5NaO2) 60 g NaOH 1,5 mol Procedure 1. mix it and crush it 2. Carry out a dry distillation of a mixture of benzoate and hydroxide 3. Pre-distill the orange liquid to produce a transparent benzene solution (benzene boils at...

Is it much work to get p2p from b-nitrostyrene? I made a bunch a while ago thinking it was nitroEthane (making p2np) but it turned out to be nitroMethane so got b-nitrostyrene, unfortunately I made a bunch like 750grams and it would kill me to throw it away. I would like to use it for...

Conversion: 1. 1kg of MAPA (Methyl 2-phenylacetoacetate) powder is dissolved in 1 liter of hot H2O with stirring 2. 3 Liters of HCL 37% are added 3. Reflux with stirring around 7-8 hours at 80-90C until the oily part seems brown. 4. Cooled in an Ice bath. 5. Now are 2 layers in the flask...

Reagents: 1-Phenyl-2-nitropropene (P2NP; cas 705-60-2) 1000 g; Methanol (MeOH) 10 L; Sodium borohydride (NaBH4) 470 g; Hydrogen peroxide (H2O2) 30% 6 L; Potassium carbonate (K2CO3) 1800 g; Hydrochloric acid (HCl) 37% aq; Dichloromethane (CH2CI2) 5 L; Sodium hydroxide (NaOH) 5 L 25% aq...

Reagents: 1-Phenyl-2-nitropropene (P2NP; cas 705-60-2) 1.63 g, 10 mmol; Powdered iron (Fe) 3 g; FeCl3 0.6 g; Hydrochloric acid (HCl 36% aq.) conc. 4 ml; Toluene 15 ml; Water 55 ml; Hydrochloric acid 3N (10.45%) HCl 25 ml; Sodium bicarbonate (NaHCO3); Magnesium sulfate (MgSO4); Equipment and...