naoh

Hi, I need help! : ) Benzoquinone Wacker Oxidation of Safrole in Methanol to yield MDP2P From Erowid.org/archive/rhodium/chemistry/wacker.benzo-meoh.html By Methyl Man Stuck on 5% NaOH Wash #2. Wash #1 was as expected, resulting in a very black top “aqueous?” layer that was discarded. When...

hello, after boiling N-formy with HCL for two hours, do we first need to separate it before we bring it to ph14 ? and when we add the NaOH, do we need to boil the solution again before washing with toluene ? Thank you