Synthesis of AMP Sulphate. Leukart Reaction
In this topic presented the results obtained in the synthesis of AMP by using Leuckart reaction.
The general scheme of the process is shown in Scheme 1.
Scheme 1
Reagents and materials
16.5 g Formamide CAS 75-12-7
21 ml 80% Formic acid
16.2 ml...
Synthesis of A Sulphate via Oxime Reduction (Report 2)
Previously, a synthesis via aluminum amalgam was carried out with a low yield of the target amine
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The...
Introduction
The topic represents a correcting errors method in a case of accidental addition of excessive amount of sulfuric acid during acidifiacation procedure. Over-acidification less than 5.5 pH cause the dissolution of the target amphetamine sulphate precipitate and spoilage of the...
Does somebody know a way to dry it faster for example less than 24h because it hurts my soul every time I synth large quantities to wait for a week or more for it to dry completely? Dessicator doesn't work for me. Rags and filter sheets take at least a week to dry it completely.
The reactions proceed according to Scheme 1.
Scheme 1.
Starting reagents and materials
5 g purified P2P (P2P obtained through the reduction of P2NP with sodium borohydride and steam distill)
4.1 g Mg
37 г H3CCOONH4 (CAS 631-61-8)
250-300 ml H2O
80 ml EtOH 88%
30 ml HAc
500 ml DCM
5+5 ml Ethyl...
The reactions proceed according to Scheme 1.
Scheme 1
Starting reagents and materials
5 g purified P2P (P2P obtained through the reduction of P2NP with sodium borohydride)
4.1 g Mg
30 г HCOONH4
10-15 ml H2O
50 ml EtOH 88%
30 ml HAc
100-150 ml DCM
5+5 ml Ethyl acetate
2-3 mL of concentrated...
I’m looking for ways to purify amphetamine paste but what is the paste is it actual amphetamine or should I look for a way to remove the amphetamine paste
its hard to dose paste because well purity is unknown most advertised as 74 percent but seems to be a lie most of the time because I can...