amphetamine from p2p

  1. MisterAnonymous

    Steam distillation of Amphetamine Freebase (A oil)

    Question 
    Hi everyone, I am not a chemist but i managed to make some amphetamine freebase from P2P but just as i purified the P2P by steam distillation i wanna purify the freebase by steam distillation. But i have a question with P2P you need to add the impure P2P with a Potassium carbonate solution and...
  2. GhostChemist

    Experimental section. The synthesis of the Amphetamine sulphate using P2P with ammonium acetate and reduction with Mg

    The reactions proceed according to Scheme 1. Scheme 1. Starting reagents and materials 5 g purified P2P (P2P obtained through the reduction of P2NP with sodium borohydride and steam distill) 4.1 g Mg 37 г H3CCOONH4 (CAS 631-61-8) 250-300 ml H2O 80 ml EtOH 88% 30 ml HAc 500 ml DCM 5+5 ml Ethyl...
  3. GhostChemist

    Experimental section. The synthesis of the Amphetamine sulphate using P2P with ammonium formate and reduction with Mg

    The reactions proceed according to Scheme 1. Scheme 1 Starting reagents and materials 5 g purified P2P (P2P obtained through the reduction of P2NP with sodium borohydride) 4.1 g Mg 30 г HCOONH4 10-15 ml H2O 50 ml EtOH 88% 30 ml HAc 100-150 ml DCM 5+5 ml Ethyl acetate 2-3 mL of concentrated...
  4. GhostChemist

    Amphetamine Synthesis via P2P Oxime Reduction

    Reactions proceed according to Scheme 1 Reagents and Materials: 8.1 g of aluminum 0.05 g of mercury(II) chloride 5 g P2P 2 g of hydroxylamine or a mixture (50-60 ml of IPA (or ethanol) + 2.5 g of NaOH + 4.55 g of hydroxylamine hydrochloride) 50 ml of ethanol 2-liter flask 2 liters of ice-cold...
Top