Hi everyone,
I am not a chemist but i managed to make some amphetamine freebase from P2P but just as i purified the P2P by steam distillation i wanna purify the freebase by steam distillation.
But i have a question with P2P you need to add the impure P2P with a Potassium carbonate solution and...
The reactions proceed according to Scheme 1.
Scheme 1.
Starting reagents and materials
5 g purified P2P (P2P obtained through the reduction of P2NP with sodium borohydride and steam distill)
4.1 g Mg
37 г H3CCOONH4 (CAS 631-61-8)
250-300 ml H2O
80 ml EtOH 88%
30 ml HAc
500 ml DCM
5+5 ml Ethyl...
The reactions proceed according to Scheme 1.
Scheme 1
Starting reagents and materials
5 g purified P2P (P2P obtained through the reduction of P2NP with sodium borohydride)
4.1 g Mg
30 г HCOONH4
10-15 ml H2O
50 ml EtOH 88%
30 ml HAc
100-150 ml DCM
5+5 ml Ethyl acetate
2-3 mL of concentrated...
Reactions proceed according to Scheme 1
Reagents and Materials:
8.1 g of aluminum
0.05 g of mercury(II) chloride
5 g P2P
2 g of hydroxylamine or a mixture (50-60 ml of IPA (or ethanol) + 2.5 g of NaOH + 4.55 g of hydroxylamine hydrochloride)
50 ml of ethanol
2-liter flask
2 liters of ice-cold...