Question Potrebujete pomoč pri povečanju obsega

[Fernandohatescorn]

Pozdravljeni vsiHočem povečati p2p na 1000 g in če bo šlo dobro, p2p na 5000 g za leuckartovo sintezo. Imam razmerja za majhno serijo. Ali mi lahko pomagate pri povečanju p2p na 1000 g. In še eno p2p 5000g, koliko vsake kemikalije bi potreboval. Hvala.

 

[HerrHaber]

Najprej boste potrebovali dovolj velik reaktor z vso dodatno opremo.

 

[Tovenaar]

Dovolj velik reaktor, dovolj velik komplet za parno destilacijo, neposredno bi povečal na 5 kg. Leuckart se lahko izvede v nerjavnem jeklu. Ko naredite drugi korak s kavstično sodo.
kupite majhen 100-litrski rezervoar, pripeljete varilca, ki vam izdela kondenzator.

 

[mycelium]

You can buy those dirt cheap now
It is called a tube in shell condenser, and that shit goes fast, as it is a bunch of condensing tubes cooled down with ice water, or, in my case, IPA and dry ice to get it below -50c. (Gets down to -78c but my thermometer doesn't go that low)
You can get one for 2k from "hardware factory store " that you don't even need a chiller or homemade chiller for, it has a big scoop for ice or dry ice.

Shit they are 1100 for a 4" diameter and 2200 for a 6" diameter, but you can scoop dry ice into the area, pour in IPA and it all gets super cold...amazing for recovery of any low boiling hydrocarbon vapor