Need help convert bmk 5449-12-7 to free base A-oil

Saul

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I know there are multible topics already but it is totaly unclear and they al say different things

cas 5449-12-7 is verry cheap and verry easy to buy

I have reseve mine but I realy need the right info .

is it possible to post this synthesis from scratch to free base A-oil

or if it is to much trouble point me to the right info plz thx
 

TJD

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Hi have you got a step by step how to turn BMK to A oil
 

Saul

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no , I dont
 

Saul

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this is an verry old topic link you provide here .
it is not useable anymore becouse off wrong info
also it is a different cas bmk.
 

Saul

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.....
 
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Wizzkid

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Apparently phosphoric acid is the best route for this cas I’m being told. Using HCL is getting very small results. Anyone with more info on phosphoric route would be welcomed ?
 

G.Patton

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Hi, Soul. Where is wrong info? You can make bmk 5449-12-7 to P2P and than to amph. What the problem? You can't understand or what? Higgs has sen't you solution.
What synthesis do you mean?
 

Wizzkid

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Just this cas into BMK using phosphoric. I understand from the link in the thread the basics but looking for ratios and times or as much info as possible
 

G.Patton

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Actually, I've never heard about method which you mentioned. Can you share your information source?
 

Wizzkid

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It’s actually all on one of the pinned threads about apaan conversion. Second from the bottom. It briefly mentions phosphoric acid conversion but doesn’t go into detail. I mistakenly said it was in this thread but I think I must of had a few threads open. Anyway after having issues with this cas I spoke to the supplier and they said using phosphoric acid will get better results than hcl.With this cas.
 

MadHatter

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But ... that's conversion from APAAN to BMK? This CAS is BMK gllycidate, is it not?
 

G.Patton

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You are right, I forgot about it.
 

Saul

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dear G.patton ,
verry sorry for the late replay I was on holiday I check now all messages and replay you after
 

Saul

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I had already found this out myself because hydrochloric acid has a much too low boiling point. formic acid also has a boiling temperature that is too low.
for this cas we need minimum 140°c so then we need phosphoric acid boiling point 150°c

this is what i meant by wrong methods and they are still online here.
 

badbreak2

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Its not needed boilingpoint 150 if you make big production just cook till its 120°c and count 6 hours Only what is important you use for 1 kg 5449-12-7 1.5L phosphoric acid 85% and 0.5 L water for each kg
 

Castlebar

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Hi Saul I've got the same product and looking for help/instructions to convert to oil how did you get on did you find the way?
 

btcboss2022

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I think don't try to search the info in the forum because I posted a detailed process to convert it that CAS to oil even videos were uploaded.
 

Castlebar

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Thanks btcboss2022 where can I find the videos please
 

Castlebar

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Thanks when I click link shows error
 
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