- Language
- 🇺🇸
- Joined
- Feb 24, 2023
- Messages
- 13
- Reaction score
- 5
- Points
- 3
Equipment needed:
1x jacketed glass reactor
1x heater
1x chiller
1x vacuum pump
1x nutsche filter
1x rotovap
How to:
1) dissolve 1:1 CBD isolate in heptane @ 80C
2) stabilize jacket temp to 50C
3) add 1% of CBD isolate weight in PTSA
4) run reaction for 3,15h after the addition of reagent (If the reaction doesn’t take off (exothermic reaction) at 50c after 10 minutes, bump jacket temp to 60c)
5) cool down to room temp
6) water washes 1:1
2x straight distilled water wash
2x natrium bicarbonate wash
2x salt wash
3x straight distilled water wash
After washes pH should be 7
7) filter heptane thru b80/celite/magsil
8) recover heptane in rotovap
9) distill crude D8 oil under full vacuum
1x jacketed glass reactor
1x heater
1x chiller
1x vacuum pump
1x nutsche filter
1x rotovap
How to:
1) dissolve 1:1 CBD isolate in heptane @ 80C
2) stabilize jacket temp to 50C
3) add 1% of CBD isolate weight in PTSA
4) run reaction for 3,15h after the addition of reagent (If the reaction doesn’t take off (exothermic reaction) at 50c after 10 minutes, bump jacket temp to 60c)
5) cool down to room temp
6) water washes 1:1
2x straight distilled water wash
2x natrium bicarbonate wash
2x salt wash
3x straight distilled water wash
After washes pH should be 7
7) filter heptane thru b80/celite/magsil
8) recover heptane in rotovap
9) distill crude D8 oil under full vacuum