This website is making great progress in synthetic videos. This video was super clear. In my opinion, the animations of bits of text and moving trash can indicating what to do with a leftover solution were clear. Keep it up.
It can be worked up from decarboxylation of Proline. There's documented information out there; however I'm not sure if there is a thread on this forum though. Maybe that'll be one of my first contributions as I've now made it on three occasions.
Can be synthed pretty easy from the decarboxing of l-proline and basic carbonate I am attempting this today proline can be found cheap even on Amazon the.whole thing only requires a simple distillation and some high Temps. Pyrrolidine is my last hurtle I have good bromo ketone choping at the bit to be animated
amazing video! Respect to its creators! in this regard, I have a question for the respected community, the fact is that I exactly followed the instructions from it, and at the very end, when I brought pH = 6, and put the vessel in the freezer, after almost 2 days I took it out and I saw that almost nothing had formed in it, except for a handful of crystals, which, when washed with dehydrated acetone, disappeared without a trace. what's the matter? what exactly did I do wrong?
Synthetics sells it on Etsy and eBay. He has hundreds of thousands of sales. A little thought and you could get it without revealing your identity and he's in Texas so no customs
Synthetics sells it on Etsy and eBay. He has hundreds of thousands of sales. A little thought and you could get it without revealing your identity and he's in Texas so no customs
amazing video! Respect to its creators! in this regard, I have a question for the respected community, the fact is that I exactly followed the instructions from it, and at the very end, when I brought pH = 6, and put the vessel in the freezer, after almost 2 days I took it out and I saw that almost nothing had formed in it, except for a handful of crystals, which, when washed with dehydrated acetone, disappeared without a trace. what's the matter? what exactly did I do wrong?
Hi.thanku for your post.sorry i do not have a well educated answer for you.i too will be attempting to carry out this synthesis as well.ive be cramming the chemistry and general chemistry behind it for months,while collecting the things needed.from a near idiots standpoint(me),if the crystals disappeared they where solublized by the solvent,the acetone.per video,a-pvp is said to be partially soluble in cold acetone.acetone is generally not very water containing ive seen.as a idiot,lol,i question where the crystals a-pvp? And was the solvent dry enough? Hope im understanding u correctly.i will follow you.best wishes.
Hi.thanku for your post.sorry i do not have a well educated answer for you.i too will be attempting to carry out this synthesis as well.ive be cramming the chemistry and general chemistry behind it for months,while collecting the things needed.from a near idiots standpoint(me),if the crystals disappeared they where solublized by the solvent,the acetone.per video,a-pvp is said to be partially soluble in cold acetone.acetone is generally not very water containing ive seen.as a idiot,lol,i question where the crystals a-pvp? And was the solvent dry enough? Hope im understanding u correctly.i will follow you.best wishes.
Hi.thanku for your post.sorry i do not have a well educated answer for you.i too will be attempting to carry out this synthesis as well.ive be cramming the chemistry and general chemistry behind it for months,while collecting the things needed.from a near idiots standpoint(me),if the crystals disappeared they where solublized by the solvent,the acetone.per video,a-pvp is said to be partially soluble in cold acetone.acetone is generally not very water containing ive seen.as a idiot,lol,i question where the crystals a-pvp? And was the solvent dry enough? Hope im understanding u correctly.i will follow you.best wishes.
amazing video! Respect to its creators! in this regard, I have a question for the respected community, the fact is that I exactly followed the instructions from it, and at the very end, when I brought pH = 6, and put the vessel in the freezer, after almost 2 days I took it out and I saw that almost nothing had formed in it, except for a handful of crystals, which, when washed with dehydrated acetone, disappeared without a trace. what's the matter? what exactly did I do wrong?
AMINATION Witam ludzi biznesu Mam pytanie. 1). 4L octan etylu 1100ml pirolidyna czy dotyczy to 1kg 2 bromowalerofenonu? 2). Zgodnie z instrukcją wideo potrzebujesz 400ml octanu etylu, 87g pirolidyny (czy 87g 110ml pirolidyny?) Czy to 87g pirolidyny to inna dawka 2bromowaleofenonu? 3). Czy mogę krystalizować z a-pvp hcl z IPA i zostawić na 3-4 dni, aby uzyskać duże kryształy? Dziękuję wszystkim, którzy pomogli
Hi to all gentlemen. while working for pvp.HCl synthesis, bromination was successful. However, during amination, color of rxn was faded and never turned back deeper after complete mixing of pyrrolidine. During crystallization, pH was made 5, but the very little crystals came out after resting for 16 hrs in deep freezer. 10 ml of valerophenone and other chemicals in proper ratio gave only 0.8 g of PVP.HCl dry crystals. Can any one identify the reason for such small product, while every step was exactly same as advised.
Hi to all gentlemen. while working for pvp.HCl synthesis, bromination was successful. However, during amination, color of rxn was faded and never turned back deeper after complete mixing of pyrrolidine. During crystallization, pH was made 5, but the very little crystals came out after resting for 16 hrs in deep freezer. 10 ml of valerophenone and other chemicals in proper ratio gave only 0.8 g of PVP.HCl dry crystals. Can any one identify the reason for such small product, while every step was exactly same as advised.
Further to this, I thought, may be my HCl was not 37% as the bottle cork was open when I found it, so the strength of acid would have been depleted. That might be the reason to use more volume of acid to reach at pH of 5 and hence more water was introduced which stopped the pvp.HCl to crystalize. Therefore I added sufficient QTY of dry acetone to lower the percentage of water in the solution. However, after putting the solution for further 16 hrs in freezer, I found no crystals but saw a thin yellow layer of unknown liquid, floating on acetone surface. I am surprised what is this. It can not the watery solution of pvp salt, as water is not only heavy than acetone and Et. acetate but also miscible with acetone. It can not be pvp free base as the pH is still near 5. Moreover, for the sake of argument, if it would be free base, it would had been dissolved in organic solvent i.e. mixture of acetone and Et.acetate. Can any friend suggest what the hell is this which is lighter than acetone, non miscible with organic solvents, neither it is water nor free base.....I m unable to understand, kindly share your valued opinion for my guidance. thanks to all.
Hello, I would like to ask for a little help because I am self-taught and I don't know anyone who is interested in this, I am asking you for help with mathematical calculations, please give me a sign if possible, I mean the amount of 2-bromovalerophenone used in the video to get Alpha-Pvp, is it the same principle as for amphetamine, i.e. 1M Bromoketone + 1.5M Pyrrolidine? it would turn out that 2-bromovalerophenone was used in an amount of about 196.61g per 87g of pyrrolidine, did I count correctly?
hello everyone I have followed the steps for the production of a-pvp but that has not happened as it should be i suspect that the videos on the internet is just shit i have followed all the steps but ghet about not at all i have invested a lot of money but in the end 0 does not happen too bad that's so it's a-pvp that's just a lie
Vapors are ALWAYS something you want to avoid inhaling when working, hence why a fume hood is good to have. If not then use a well ventilated area or be creative. Safety first
Did you guys know what valeraphenone comes from valeric acid ( of course you did) BUT DID YOU KNOW THAT VALERIC ACID COMED FROM THE PLANT VALERIAN? Valeria officianalis It's an invasive species in the United States and is common in Europe and Asia. People sell it dried in bulk on the internet.
Did you guys know what valeraphenone comes from valeric acid ( of course you did) BUT DID YOU KNOW THAT VALERIC ACID COMED FROM THE PLANT VALERIAN? Valeria officianalis It's an invasive species in the United States and is common in Europe and Asia. People sell it dried in bulk on the internet.
Your information is amazing.
I found valerufonone on one of the sites, but it is risky to buy it, because I think everyone knows that valerufenone is only for alpha.
What do you think ?
Your information is amazing.
I found valerufonone on one of the sites, but it is risky to buy it, because I think everyone knows that valerufenone is only for alpha.
What do you think ?
It's less obvious if you call it p
2-bromo-phenyl-pentan-1-one
It has also been used in the synthesis of various heterocyclic compounds, such as pyridines, pyrimidines, and thiophenes. Additionally, 2-bromo-1-phenyl-pentan-1-one is used in the synthesis of polymers, such as polyacrylonitrile, polyvinyl chloride, and polyethylene
It's less obvious if you call it p
2-bromo-phenyl-pentan-1-one
It has also been used in the synthesis of various heterocyclic compounds, such as pyridines, pyrimidines, and thiophenes. Additionally, 2-bromo-1-phenyl-pentan-1-one is used in the synthesis of polymers, such as polyacrylonitrile, polyvinyl chloride, and polyethylene
I'd love to get syth for MDPV, is it muchore complicated that a-pvp? Also how necessary is the recrystallization processes? Wouldn't the HCl be more suitable for IV use?
I tried to buy from this guy and he laughed at me insulted me and said he was going back to bed. In China, turds sell precursors, but they actually don't. Made me tell him the CAS
I'd love to get syth for MDPV, is it muchore complicated that a-pvp? Also how necessary is the recrystallization processes? Wouldn't the HCl be more suitable for IV use?
I tried to buy from this guy and he laughed at me insulted me and said he was going back to bed. In China, turds sell precursors, but they actually don't. Made me tell him the CAS
I believe it is exactly the same procedure using methylene-dioxy pyrovelarophenone < a-bromo-methylenedioxy-pyrovelaraophenone<MDPV< I
These people sell pretty much everything under the sun. They're basically the Amazon of China. So you can expect them to know everything about every item. But you do make a valid point.
BTW have you looked at polish vendors for precursors
These people sell pretty much everything under the sun. They're basically the Amazon of China. So you can expect them to know everything about every item.
Yeah ok you have a point. They also don't always stock stuff like a pvp but remember what the penalty for drugs in China is. But yeah if the dude laughed at you he's am asshole and unprofessional. Font you fare buy from him and give him the satisfaction..
Are u in the eu or basically why order from China? U could lose it at customer and it will take ages to arrive
Yeah ok you have a point. They also don't always stock stuff like a pvp but remember what the penalty for drugs in China is. But yeah if the dude laughed at you he's am asshole and unprofessional. Font you fare buy from him and give him the satisfaction..
Are u in the eu or basically why order from China? U could lose it at customer and it will take agr
I'd love to get syth for MDPV, is it muchore complicated that a-pvp? Also how necessary is the recrystallization processes? Wouldn't the HCl be more suitable for IV use?
@NinjaFlakkaZombie Well because Chinese vendors advertise it at prices so low that it's impossible to look away. They no longer offer it for sale in the open forum but if you pm them, they offered it to me for about $125/kg (2-bromo-4-methyl-1-phenylpentan-1-one) and $115/L for the pyrovelarophenone equivalent. I wouldn't accept anything illegal from China. The risk is astronomical in my opinion. I have bought it off of a major online marketplace, received it, sent from inside the USA, with no fanfare, no questions were asked and it's been 2 months and is long gone from my possession. It was expensive compared to Chinese prices. Basically $4/g.
The person is either licensed to receive such things ( the DEA does issue paperwork for businesses to have things of the nature), in a position to procure them with little risk ( such as the faculty of a University department licensed to possess it)or has put a lot of effert into obscuring his identity through incorporations business licensing and mail forwarding
My sample of MDPV was made from bromo-MDP1P obtained state side from a VERY POPULAR WEBSITE! now did i pay with my first borns soul for a very small amount well yess but it’s rather nice and pure bromoketone.
I totally agree I've talked to so many chibese vendors but then my senses get the better of my.. keep that shit discrète. Prison is boring and lawyers arent cheap. I'm currently waiting for something from china (very small quantity and reputable vendorbalso not cheap but cheap for what it is). If ur buying precursors tho keep that shit as close to home as u can and if u buy from china im learningvthe value of patience but im gonna end up dailing the course haha
@NinjaFlakkaZombie Well because Chinese vendors advertise it at prices so low that it's impossible to look away. They no longer offer it for sale in the open forum but if you pm them, they offered it to me for about $125/kg (2-bromo-4-methyl-1-phenylpentan-1-one) and $115/L for the pyrovelarophenone equivalent. I wouldn't accept anything illegal from China. The risk is astronomical in my opinion. I have bought it off of a major online marketplace, received it, sent from inside the USA, with no fanfare, no questions were asked and it's been 2 months and is long gone from my possession. It was expensive compared to Chinese prices. Basically $4/g.
The person is either licensed to receive such things ( the DEA does issue paperwork for businesses to have things of the nature), in a position to procure them with little risk ( such as the faculty of a University department licensed to possess it)or has put a lot of effert into obscuring his identity through incorporations business licensing and mail forwarding
In in the eu and if im hetting precursors theyre coming from an eu state for sure. We dont have a real comparison to the dea but still. Precursors and drugs.. diffenrent ballgame...fuck that its a different sport entirely. I think ull br ok with an ounce of pvp from china (not legal advice) 2-bromo on the otherhand they will envie you tp to there hôtel room. Net tging u kboz the bathrobe slifndes iff revealing the long yard Dick of the law and ull take all of it. U guys (I'm American too just dont live there take the war on drugs so seriously and enforce it and prevent it in the dumbest ways imaginable... never buy non domestic precursors
i have felt every MM of the US justice systems yard long unit all for a used weed pipe that was full of dirt (left in fishing bag) they will charge you with eq sentecne of 100kg marrijunna for every gram of bromo compound which they will first convert in there wacky coke indude delerium to cocaine and then for every gram that come up with will be the same sentencing guideline as 100kgs of weed if your gonna play there game gotta be ready to pony up for a real good lawyer
🫨 Jesus man, you had me scared for a second, then I realized that you are just a tad dramatic. To be fair the police and government in general are a bit dramatic. So you're with the government you say? I know there's enough hoops to jump through and walls to hide behind that a person could have a package intercepted and evade identification, but the amount of effort it takes is more than the amount of effort it takes to synth 4-mmc starting from valerian roots or mdma from Sassafras bark. None of these things am I capable of not do I think I can learn them in the amount of life I have left. I would much rather just buy drugs but the quality is so low where I'm at that one can hardly extract or purify it to a usable level. It doesn't even matter if you buy expensive or cheap drugs, they're all neutered.
🫨 Jesus man, you had me scared for a second, then I realized that you are just a tad dramatic. To be fair the police and government in general are a bit dramatic. So you're with the government you say? I know there's enough hoops to jump through and walls to hide behind that a person could have a package intercepted and evade identification, but the amount of effort it takes is more than the amount of effort it takes to synth 4-mmc starting from valerian roots or mdma from Sassafras bark. None of these things am I capable of not do I think I can learn them in the amount of life I have left. I would much rather just buy drugs but the quality is so low where I'm at that one can hardly extract or purify it to a usable level. It doesn't even matter if you buy expensive or cheap drugs, they're all neutered.
this is very true but having a cheap uncut substance is whole different world from street grade. one that i did not discover untill chem came in my life but its been a life time devotion tho and a huge invesment . i sleep well at night knowing what serve is free from toxic cuts and fillers and one less persson that gonna die from fent
Haha yeah totally with the government. I spent a year doing surveilance of a prison cell well.a couple months to honest
Tho actually it's nor.dumb to think this way, the cops come after clients too depending on products bought and location (let's.fscw it sereot7ped.dxist for a reason Anand yea police are very terrified of riding in cars or doing too.much nkn work.work.
It's best not go trust.anyonr here
He'll even.heisenberh could br a cop... it's unlikely but.as an example it's just u never know so I get.pissef of when.some guy who barely understands what I'm telling him is offering a.conversation which includes my shipping address
I'm not a chemist yet and.altho I've done my research and felt is less.dsnhetous for.me.. instil would never work withnut. I remember my would sleep over a day from 0.5 of Xanax and felt hot.pocks too. It's.a.baf idea tonwork.with that.. at the.momenr I always bumpy my at a place that doesn't serve. Wrl but they don't cut... I. Belgium that basically means they are selling what u buy .in Columbia and their smaller bags I.male be getting a little ripped fmodf burning put this stuff.in my veins so... nomquestion from weed to xtc ALWAYS choose qualityband then work on it creasing production. Iioking forward.to my first Cookson. Much nut inkniq I.wont gave great product nut my goal I'd finnishingneijt A-one predilection.. incan worf with that and get better
Haha yeah totally with the government. I spent a year doing surveilance of a prison cell well.a couple months to honest
Tho actually it's nor.dumb to think this way, the cops come after clients too depending on products bought and location (let's.fscw it sereot7ped.dxist for a reason Anand yea police are very terrified of riding in cars or doing too.much nkn work.work.
It's best not go trust.anyonr here
He'll even.heisenberh could br a cop... it's unlikely but.as an example it's just u never know so I get.pissef o
Most of that I Can't understand but the government thing was a joke of course and yes it's hard to remove adulterants sometimes impossible and an uphill battle because you usually don't know what they are. I pay top dollar for drugs but even then I rarely get high purity. A couple years ago I reliably got cocaine that titrated to 78% for $350/3.5g. it was the best stuff around, every one agreed. I paid the same price for the same amount of what was supposed to be crystal mdma a few months ago and I go purple crushed powder. It tested positive on 2 tests but it took 600 mg to get high on
where i am from you 350 for a cut and your lucky if its 10percent (good stuff) is lucky to break 20 its very bad.I have seen that purple powder making the rounds i wonder if the there a small amount of mdma in with a analog i have seen many snyths from sas to pmk and never did i see some out purple like that maybe shades of purple but good mdma should be a stunning sparkly crystal and never take 600mg i rateher bk-md at that point
where i am from you 350 for a cut and your lucky if its 10percent (good stuff) is lucky to break 20 its very bad.I have seen that purple powder making the rounds i wonder if the there a small amount of mdma in with a analog i have seen many snyths from sas to pmk and never did i see some out purple like that maybe shades of purple but good mdma should be a stunning sparkly crystal and never take 600mg i rateher bk-md at that point
Well I took 300 and an hour later another 300. There's a mountain of purple pressies going around right now that people are warning about being so strong, and I think the guy probably just crushed those up and sold them. I'm thinking 6 pressies=3600 mg and has an actual 1800mg of MD in it. You know bk-mdma becomes regular mdma in 1 reaction. I want to say a Wilkinson, but I didn't look it up
@NinjaFlakkaZombie Well because Chinese vendors advertise it at prices so low that it's impossible to look away. They no longer offer it for sale in the open forum but if you pm them, they offered it to me for about $125/kg (2-bromo-4-methyl-1-phenylpentan-1-one)
This is not true?! Do you know HOW many times I was asking for 2-bromo-4-methyl-1-phenylpentan-1-one AND NOBODY had it.
No, only everyone wanted to sell all kind of other chemicals with 25kg MOQ.
This is not true?! Do you know HOW many times I was asking for 2-bromo-4-methyl-1-phenylpentan-1-one AND NOBODY had it.
No, only everyone wanted to sell all kind of other chemicals with 25kg MOQ.
? What risk do you have if you don't order something on your real name and address?
I'll screenshot the convos if you insist, I've gotten 5 quotes for both. I can't show you Precursor-supplier's because he has auto self destruct on his telegraph.
You risk your freedom. Did you think that they realise the name is fake and say fuck it? They could put a tracker the size of a grain of rice right into the corrugation of the box and watch you take it somewhere and then surveill that place and wait until you try to use it to kick the door in. They could deliver it to the address and fly a drone over it in a pattern 2 miles up and wait for you to try to collect it. I can think of at least a couple of other things they could do.
You haven't thought this through. You aren't going to maintain your freedom for 6 months if you don't consider the manpower money and technology the DEA has.
This is not true?! Do you know HOW many times I was asking for 2-bromo-4-methyl-1-phenylpentan-1-one AND NOBODY had it.
No, only everyone wanted to sell all kind of other chemicals with 25kg MOQ.
? What risk do you have if you don't order something on your real name and address?
Yeah I got quotes in the $125/kg range and $80 shipping. Id pay 3x that without batting an eye if it was sent domestically. I actually spent a shitload on some domestically. $200 for 50 grams and I'll do it again soon so if you are legit and can beat that price. I know a buyer
Lookchem Provide Cas 33809-96-0 Basic information: structure,molecular formula,safety information, MSDS, technical documents, related articles, process route, Upstream and downstream products & more at Lookchem. We also Provide suppliers and manufacturers and reference price for 33809-96-0.
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I really can't understand the euphoria here. The end product looks terrible and the impurities are visible to the naked eye. I wouldn't even take this if I were paid for it.
The cleaning of the intermediate product and the free base is supposed to be a joke.
Why does everything always have to be quick and dirty?
As Uncle Fester once said: If you put shit in, you get shit out. Regardless of whether it is psychoactive or not.
I really can't understand the euphoria here. The end product looks terrible and the impurities are visible to the naked eye. I wouldn't even take this if I were paid for it.
The cleaning of the intermediate product and the free base is supposed to be a joke.
Why does everything always have to be quick and dirty?
As Uncle Fester once said: If you put shit in, you get shit out. Regardless of whether it is psychoactive or not.
I was confused about which thread we were in. I actively comment in about 10 ongoing threads about 2-b-4-mp. I think you asked me what chemical I was referring to and I responded 14551-82-7, you should have realized that no? I do drugs bro. I got confused
I really can't understand the euphoria here. The end product looks terrible and the impurities are visible to the naked eye. I wouldn't even take this if I were paid for it.
The cleaning of the intermediate product and the free base is supposed to be a joke.
Why does everything always have to be quick and dirty?
As Uncle Fester once said: If you put shit in, you get shit out. Regardless of whether it is psychoactive or not.
Yeah I got quotes in the $125/kg range and $80 shipping. Id pay 3x that without batting an eye if it was sent domestically. I actually spent a shitload on some domestically. $200 for 50 grams and I'll do it again soon so if you are legit and can beat that price. I know a buyer
Yeah ok you have a point. They also don't always stock stuff like a pvp but remember what the penalty for drugs in China is. But yeah if the dude laughed at you he's am asshole and unprofessional. Font you fare buy from him and give him the satisfaction..
Are u in the eu or basically why order from China? U could lose it at customer and it will take ages to arrive
China manufacture must of chems and outsource the APVP on Vietnam (india). I am finding put a police-hunted former China-manufacturer; now turned turned to trading narcs from Vietnam Mexico Paraguy Usa. Lowest price possible. I just have to get what I ordered. All narc-parcels are from eu/china they all gone straight to me-eu. You get scammed until you get the dream drug deal
Yeah ok you have a point. They also don't always stock stuff like a pvp but remember what the penalty for drugs in China is. But yeah if the dude laughed at you he's am asshole and unprofessional. Font you fare buy from him and give him the satisfaction..
Are u in the eu or basically why order from China? U could lose it at customer and it will take agr
Beacuse when you find The delivering shady trade company; you struck gold... I know that for sure. Just keep on looking for it, China is so big and have outsourcing to other countries. Or buy from me here when time comes. CHINA IS THE GOAL...dont you forget the source. CHINA GOT IT
This myth is unreal about
CAS 33809-96-0 + CAS 123-75-1 => A-pihp.
While there are reports about CAS 59774-06-0 actually being used in producing A-php (same way as A-pvp), it seems not possible with CAS 33809-96-0 to produce A-pihp.
Why? Because nobody can deliver 33809-96-0. So it must be another way.
Maybe A-php can be changed into A-pihp (nothing less than a isomer).
"Maybe A-php can be changed into A-pihp (nothing less than a isomer)."
APHP PV7 is stronger better than APIHP (APHP is a skewed equal to APVP) and sells for sure more money. I always wonder why many don't think so, and your wish is the utter downgrade handicapping of the hard hitting entact stim APHP I respect your view. Good to hear real horror show
This myth is unreal about
CAS 33809-96-0 + CAS 123-75-1 => A-pihp.
While there are reports about CAS 59774-06-0 actually being used in producing A-php (same way as A-pvp), it seems not possible with CAS 33809-96-0 to produce A-pihp.
Why? Because nobody can deliver 33809-96-0. So it must be another way.
Maybe A-php can be changed into A-pihp (nothing less than a isomer).
u should be just able to take 4-Methyl-1-Phenylpentan-1-One ( CAS: 2050-07-9 , seems to be pretty obtainable anywhere around the globe) and brominate it yourself to get the desired 33809-96-0 and proceed with the rest of the recipe, definitely easier way than to mess with the A-PHP molecule to create an isomer i think
APHP PV7 is stronger better than APIHP (APHP is a skewed equal to APVP) and sells for sure more money. I always wonder why many don't think so, and your wish is the utter downgrade handicapping of the hard hitting entact stim APHP I respect your view. Good to hear real horror show
APHP have lower dose etc so it is stronger in all, stronger than APVP, and most see it so, even if not DAT. Dont know what DAT is. APIHP is rather strong and nice but I got bored I had unlimited supply. APHP only little I used and cannot say for sure about it-
ECHEMI -- The name is originated from the abbreviation of “E-commerce of chemical”. ECHEMI is a chemical supply chain service company headquartered in Hong Kong, providing chemical raw materials supply, research and analysis, marketing, distribution, logistics and E-commerce.
I couldn't get the hexanophenone to react as readily as valerophenone when I tried it. Same set up. In my case was just missing the reflux condenser but I made sure it was as close to sealed as I could. The problem arose when dripping in the pyrrolidine. It didn't react very well even under very vigorous mixing in ethyl acetate. The free base aPHP itself dried off was not very active let alone when I hit it with some HCL. Ended up with a bunch of ALMOST inactive powder even after washing it. It was somewhat there but barely. I'd have to say only very little of it actually reacted if any. It ended up being just very weak and disappointing. I may not be able to acquire valerophenone again so it's sad to think I may not be able to do this again. Lmk if heat or a more preferred set up may help more.
Does anyone know how to synth MDPV? Is it just Apvp done with methylamine? I have made both aphp and apvp but never mdpv and would like to know if I could go from 2-bromovalerophenone to MDPV or is the process completely different
I have no measurements in my Vevor stirrer. How do I know if my stirrer is too fast or slow, man ... And is the stirring speed THAT critical, to mess up the whole work? I want to know.
I have no measurements in my Vevor stirrer. How do I know if my stirrer is too fast or slow, man ... And is the stirring speed THAT critical, to mess up the whole work? I want to know.
