Question Nepieciešama palīdzība

Fernandohatescorn

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Sveiki visiEs gribu palielināt p2p līdz 1000 g un, ja tas izdosies, p2p līdz 5000 g leikarta sintēzei . Man ir koeficienti mazām partijām . Vai jūs varētu man palīdzēt ar p2p palielināšanu līdz 1000g. Un vēl vienu p2p 5000g, cik daudz katras ķīmiskās vielas man būtu nepieciešams. Paldies.
 

HerrHaber

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Vispirms jums būs nepieciešams pietiekami liels reaktors ar visiem tā piederumiem.
 

Tovenaar

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Pietiekami liels reaktors, pietiekami liels tvaika destilācijas komplekts, es tieši palielinātu līdz 5 kg. Leikartu var veikt nerūsējošā tēraudā. Kad veicat otro soli ar kaustisko sodu.
iegādājieties nelielu 100 l tvertni, novadiet metinātājam, lai viņš jums izgatavotu kondensatoru.
 

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mycelium

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You can buy those dirt cheap now
It is called a tube in shell condenser, and that shit goes fast, as it is a bunch of condensing tubes cooled down with ice water, or, in my case, IPA and dry ice to get it below -50c. (Gets down to -78c but my thermometer doesn't go that low)
You can get one for 2k from "hardware factory store " that you don't even need a chiller or homemade chiller for, it has a big scoop for ice or dry ice.

Shit they are 1100 for a 4" diameter and 2200 for a 6" diameter, but you can scoop dry ice into the area, pour in IPA and it all gets super cold...amazing for recovery of any low boiling hydrocarbon vapor
 

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