Question Reikia pagalbos plečiant

Fernandohatescorn

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Sveiki visiNoriu padidinti p2p iki 1000 g ir, jei tai pavyks, p2p iki 5000 g leukarto sintezei. Turiu mažos partijos santykius . Ar galėtumėte man padėti padidinti p2p iki 1000g. Ir dar vieną p2p 5000g, kiek kiekvienos cheminės medžiagos man reikėtų. Ačiū.
 

HerrHaber

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Pirmiausia jums reikės pakankamai didelio reaktoriaus su visais jo priedais.
 

Tovenaar

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Pakankamai didelis reaktorius, pakankamai didelis garų distiliavimo rinkinys, aš tiesiogiai padidinčiau iki 5 kg. Leukart galima daryti iš nerūdijančio plieno. Kai atliekate antrąjį žingsnį su kaustine soda.
nusipirkite mažą 100 l talpyklą, leiskite suvirintojui padaryti jums kondensatorių.
 

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mycelium

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You can buy those dirt cheap now
It is called a tube in shell condenser, and that shit goes fast, as it is a bunch of condensing tubes cooled down with ice water, or, in my case, IPA and dry ice to get it below -50c. (Gets down to -78c but my thermometer doesn't go that low)
You can get one for 2k from "hardware factory store " that you don't even need a chiller or homemade chiller for, it has a big scoop for ice or dry ice.

Shit they are 1100 for a 4" diameter and 2200 for a 6" diameter, but you can scoop dry ice into the area, pour in IPA and it all gets super cold...amazing for recovery of any low boiling hydrocarbon vapor
 

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