4mmc problem

mariola12

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hello i tried to make 4mmc exactly like in this video http://bbzzzsvqcrqtki6umym6itiixfhn...n/media/mephedrone-hydrobromide-synthesis.57/ but something goes wrong and I can't get the final result. In first phase everything is good I have got oil(RM) but when I add Hydrobromic acid it's start the crystallization of mephedrone salt(I think too soon) and the mixture don't change like in video at 3:19. It have got still crystal clear red color, pH is about 5-6 and even if I put it to the freezer the color is still red not like in video at 3:41. Could someone tell me is that salt on the bottom of beaker is good or it is something else if I did not have color change in the mixture? Does the ambient temperature affect the mixture?
 

dre

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U need heat it and much liquid must get out then
 

dre

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And u dont wash freebase good then your liquid is red
 

Huey Freeman

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in acidification phase you should add the acid drop by drop and a salt must form on every drop until the ph is 5.You take out the salt and recrystalize it.Red color occurs when you put too much acid at once(at leas for me)
 

dre

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Can put all acid and good mix the same effect i do like it and get mmc later freezer and is finish
 

Huey Freeman

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That s how i fucked up a few batches...If you are new to it take ur time with acidification or you could burn up some nostrils
I did my synthesis in DCM so the colos could differ.
As long as the salt is formed with the right PH you can filter it and recrystalize it.
 

dre

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I made it long time now is cold i made outside and all work good
 
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