I need some help MDMA Freebase Oil

[bitcoinup2020]

I need some help

I do mdma synthesis using the Leuckart method. I can produce MDMA Freebase but the oil is brownish black. I checked with the MDMA urine test kit. This has a positive effect.
but the problem i encountered is I can't purify MDMA Freebase oil.
I heated it up until the temperature in the thermometer was 150 degrees but this thing didn't boil. I used a vacuum pump and couldn't get the oil out.

I want to know how to fix this problem. Anyone else having the same problem as me?

thanks for the answer

 

[chemistry.mob]

from where u bought the chemical precursors for the ectasy syntesis?

 

[2-79-790125]

how did you end up resolving this?

 

[CCL4 huffer]

hm ig extract it a few times and treat it with charcole and if it needs sum help cristalising just scratch the botom of the container